Part 2 of an impromptu play with Dave's Wekomm 10K Transfer Resistance Standard.
Was the Keithley DMM7510 multimeter the culprit in the discrepancy in the thermal response?
Dave finds out with the help of a thermal chamber.
Part 1 is here: https://www.youtube.com/watch?v=dIXbjNb82xk
http://www.wekomm.de/metrologie_e.php
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Hi In a previous video, you saw me have a little play around with a week on a 10 K laboratory resistance transfer standard that I've got hooked up to. my Keithley DMM 7510 multimeter here is just having to play around and we noticed some drift in the reading up here and I said I'd do a second video where it actually put the resistance standard inside my thermal chamber here and that's what I've done overnight. so let's take a look at what I got when I came in this morning. Now if you haven't watched the previous videos, I won't go through the data again so this won't might not make much sense.

So click here and watch that one first before we continue. Let's go. Ok, so basically nothing has changed in the setup here except I've put my weak on resistance standard inside my thermal chamber here I've set it to out 20 degrees. it shows 19 degrees up there, but I've actually got my thermometer here.

it's currently it's a well 19.8 nineteen Point six something like that. So it's been like that overnight and I've basically just been not continuously recording here although there was a where I disconnected the thing so I could put it through the port on the side here. and yes, as his standard industry practice for our thermal chambers. I've plugged it up with a rag Beauty works every time, no worries.

So yeah, and so there was a little glitch in there when I disconnected, but I've continued the data because I thought that might be valuable rather than just started again and look for stability because we've already got that. You know previous history I Wanted to carry on from the previous video so let's take a look at the data now. The data we got up previously showed a point double-o-double O 600 difference between what the resistor datasheet here tells us or what the resistor calibration sheet told us and what we actually measured on the meter head and my guess was that that point double-o-double O 600 k discrepancy was coming from the actual Keithley multimeter itself up here and we had a look at the specs for that and it seemed the temperature coefficient for this meter on its resistance range and that you know it seemed to be accountable. In fact, the datasheet value of 2.5 ppm per degree C So for a four degree C difference we're looking at actually seem to be larger, so it seemed you know it just as a rough order seem to be better than the spec, but the spec of this meter could certainly account for that.

hence why today I've actually got the resistance standard in the thermal chamber so that we can ensure that the resistance standard stays at a constant temperature and the only thing I'm going to change now is the temperature of this meter by changing my aircon here in the lab. So at the moment I'll show you what we did last night. this is where I started last night basically and see that big dip In there that was when I actually disconnected the contact. So it's good that it didn't actually give a reading outside of that I really like that and like mess up your data although it does show a little tiny red dot in there I'm not sure if you can see that but it that indicates that I Guess there was an error condition like it actually went open because we're using four terminal resistance measurement here.
Anyway, look the first thing you notice is you get we get a hell of a lot more noise on here. Look at that to what we got previously and that's not surprising. We've got this thermal chamber which uses a DC to DC converter in it to drive the Peltier device to, you know, keep it stable temperature and we've got unshielded shouldn't touch them Unshielded test leads on here, you know, so it's not the best setup so maybe we should actually turn the filter on for this one because we didn't need it before. but now that noise is getting massive.

but anyway, you could see it dropped up here when I left last night actually had the aircon on. This is when we ramped the aircon back up and we could actually see the difference. Yeah, we could actually I believed that we could actually see the oscillation of my aircon in there. You can see that like that.

And basically what I did is I turn the air con off I probably maybe I turned off well and I probably kept going anyway I turned it off before I went home. Okay, so there's no longer any aircon cycling okay, but we are getting look. we are getting some noise so you know that's like periodic noise on there, so that's rather interesting. So I don't think that's the Peltier device in the chamber.

Switching off and on. The thermal response of the resistance standard wouldn't be anything like that. You know it wouldn't be anything near that quick. So yeah, that's probably just you know, maybe switching crap from the DC to DC converter in the thermal chamber.

So when I went home last night it was I had the aircon on to ramp up like that and then it got to it was about 22 degrees or there abouts. then I went home, turn the air con off and you can see that we've got a negative temperature coefficient. As the temperature increased, we can see the change there and it's currently 26 and a half degrees in here. Let's just call it 26.

So we got that four degree differential that we had before which is handy and and once again, the temperature in the resistance standards been constant. although there might have been a little bit of thermal lag in there just to bring that up to temperature, but you know, still, it stayed stable all overnight. So really, the only change would be due to the meter here the Keithley meter. So we're because we in the previous video we suspected this meter had a negative temperature coefficient.

The datasheet doesn't tell you that, it just says plus/minus right? It doesn't tell you what the actual temperature coefficient is so, but we realize that it must have been negative. That was our theory anyway. So that was our hypothesis and so it's going negative like this. Exactly what we expected.
So let's get the difference there and there and see. You get the values and see if it's equal to that point. Double-o-double Oh 600k Discrepancy that we got last time and we can do that by going into our reading table here. So I'll read off that figure.

Point 10 Point Double-o-double Oh say Four zero and then we'll get this value at the end here and right at the end there getting basically put Nine Point Nine Nine Nine Nine Eight You know, Eight One, something like that eight - So last time we had that discrepancy as I said of the meter - what we got from the resistor Cal sheet here and we had a point: Double-o-double Oh Six Zero Zero basically difference there. So we had that discrepancy which our hypothesis was that it was caused by the temperature coefficient of the Keithley multimeter. And what did we get when we only change the temperature of the Keithley multimeter today? A difference? A Delta point Double-o-double Oh Five Nine, let's call it six Zero. We see these all make practical e the exact difference there.

and we're not even using a really, you know, decent, you know, like really controlled proper setup here. Yet we were able to convey ceccolini difference between these two. Neat beauty, huh? So what we're going to try and do now is I'll turn the air con back on. Okay, Oh, of course our temperature chamber is going to stay exactly the same temperature.

It's not. You know it can easily ka, you know, cater for external whites, low external temperature changes caused by the aircon. No worries, see our resistance standard. It's going to stay at our constant temperature which is currently.

Come on. you can do it. You know, twenty odd degrees it you know it's going to be cycle. You know, maybe half a degree around that or something like that.

so there's not much in that and I'll put turn the air con back on. it is currently twenty six degrees and I'll I think I'll turn some filtering on just so that we get a filtered signal there because that's too much noise Anyway, because we now have confirmed that this thing has a negative temperature coefficient. If we drop the temperature back down to 22, then we expect this to rise up. Let's see if we get it.

Actually I could have sworn I heard the filter turned off, but I actually have the filter turned on with the in power line cycles. Oh geez. Anyway, so it looks like we're not going to filter that any better and I don't want to go touching the setup and you know, shielding the leads and doing everything else so you know. Let's just go back to the graph and just simply turn the aircon on anyway we can see.

Even though we've got a lot of noise there now, we can see, we should be able to see that change. So I expect that now to start ramping back up. I'll give it an hour and or two and we'll come back. And I think as we saw in the previous video, I just started, it's been like five, ten minutes or something.
just started turning on the air corners. Of course you'd expect it to go immediately up in value because the temperatures coming down right the air. Khan's I've measured the temperature. you know at the vent it's pumping out like you know, 13 14 degrees C air right? So you'd expect it to go immediately up, but it doesn't.

It looks like it, just like it's not the correct term, but it's sort of like under shoots like that and then it's going to go back now. I Suspect that's because of the control loop for the reference inside the Keithley meter actually trying to. You know either the thermal response of the you know the the heater in there for the reference or you know However, they've got that control loop set up so that's probably a response from that and you know it would be nice if we had a nice noise rate. You know you could do it better if we actually put had the meter in a thermal chamber everything else and we're just measuring a fixed resistor with no noise or whatever.

You know you'd be able to see that, but you can actually see that dip go down and now it'll You can actually see it. It's starting to head back up and I believe Over the next hour or so it'll shoot right back up. So that's rather interesting that we could actually see that it's another five minutes later or something and you can see it is actually heading up there. And of course we've already hit.

you know, near our 22 degrees there. So because the ambient air is just circulating around but it hasn't immediately shot back up because there is going to be some thermal lag for the for the air to actually get in through. you know, the vent holes and this things hot inside and and it's got its own thermal characteristics inside. so it's going to take some time for this thing to actually ramp back up.

Okay, it's been an hour or so and yep, you can see that we're getting basically the same ramp we got here. not quite as big or instant because well, where rub you know we've got that extra noise on there now. and I guess the resistor wasn't adding on because it is a quarter of the value that we had before. So now we haven't got that so.

but it's slowly ramping up as you can see and it'll most likely get back to that average value that we saw there. Absolutely no doubt. And yes, I have been monitoring the temperature in side this thing and inside the thermal chamber and it has been, you know, stuck around 20 plus minus 0.5 So the thermal chamber was doing the business and keeping that even though the air kind of ramped down by four degrees because it's 22 degrees in here now the resistance standard stayed at that temperature. So what we're seeing there is just the Keithley meter and here you go, you can see that we've actually flattened out and we haven't quite come back to the peak there.
If we have a look we've come back to is that it's that straight there we go, we've cut well, almost almost pretty darn close to it. But of course as I said, there would have been some settling there of the resistor in the thermal chamber as well. So you know, maybe that and that sort of exact in quote marks figure we got a point double O double O 600. That difference we measured it might be you know it's gonna be slightly out, perhaps.

but anyway, you can see That it has recovered there, so no problems whatsoever. Look at that. So this Keithley DMM 75 one zero on the resistance range has a negative temperature coefficient and it matters. You can actually see it in the data which is really really interesting.

but look at that. look at that cycling there. There is definitely definitely cycling in that well have to get a a time period on that You can see that's actually 200 seconds or there abouts per division. So it's nice that actually tells you that.

And we're looking at basically one cycle. Um you know around about I just over two divisions. There may a bit more like it. I Think it actually varies.

It's gonna vary a bit, but that's you know. Let's say you know 400 to 500 seconds per cycle. So it might be tempting to think that this is the cycle of the aircon because it does seem to match the time period of the aircon cycling off and on. but it's not I've actually switched the aircon off at the moment.

so there is no that the you know cycle of plus minus 1/2 degree air. actually you know doing anything. So what I'm gonna do now is just last thing is just turn the thermal chamber off and I won't open. I Will just turn it off and see what happens And there we have it.

I Switched off completely and disconnected the mains power cord from our thermal chamber. I haven't opened it so the temperature hasn't changed so it looks like, well, you know you could say that that's a temperature cycle change with inside the thermal chamber, but I don't necessarily hear it actually. you know, changing that quick or though you know it could be. But as I showed in the previous video inside the thermal resistance chamber, it has a high, you know, like it's gonna have a very big thermal lag, So I'd be very surprised if it could actually change that quickly.

although it possibly could, so we might be able to see a smaller term change ie. that one quarter which we're looking at before. I'm not going to go any further in this and muck around with it, but suffice it to say that that's switching does certainly come from the thermal chamber. So there you go.

I Hope you found that video rather interesting. It started out as a quick thing I wasn't even going to make a video and I just wanted to, you know, plug that reference in overnight and I see what happened? It's turned into a two-part video getting a you know, a fair bit of data here, but it's interesting to note that that Keithley meter we've proven actually has a negative temperature coefficient substantial. one or one. that's You know, it's still within spec.
Everything we're seeing here is still within spec of the instrument. But because we're measuring right down in the noise, we can actually see the changes in the temperature coefficient, so it's rather interesting. We can see the thermal lag in there as well, you know? So if the Keithley instrument and the reference heater and other things inside, we can see that little undershoot there. and it's you know thermal response of the reference? That's all.

It's all rather interesting stuff, and this was pretty much a hack together test as I went along. I didn't you know really? design it from the start to make you know to do a proper test or still able to get some real numbers out of that that actually matched up. Fascinating stuff. So if you like that, please give it a big thumbs up.

It's another 20 minutes of waffle and anyway, I think some people might really find that rather fascinating. And if you've got you know, a decent meter with this sort of resolution, you can, you know, do and play around with that test like this. Of course you know, like all you need to do is put like a resistor short you know, straight in the input terminals for example, or a battery voltage. you know, just hook a battery straight up to it.

you know, so you don't get noise and everything with the cables and test system and all that sort of jazz so you know and you can eliminate noise and you can actually start seeing drift in your actual meter so you know. it's It's handy to know when you're doing precision measurements like this. you can't just magically take the meter and you know it's within spec. You know, plus -5 degrees outside that? okay, but within plus -5 degrees of the temperature was calibrated that it's spot-on Well know the thing, Drifter all the time.

So there you go. I Hope you enjoyed it. Catch you next time. Just a very quick follow-up I left this running over Christmas time.

it's now Boxing Day I Came back in the inside the chamber I switched it off twenty five and a half degrees and inside the lab here haven't been to the lab for like you know, a day and a half. two days or whatever. So if 25 odd degrees and this is the response I Got over that time so the aircon is definitely off, everything's switched off and there we go, but it's fascinating. You can see that's reached a new low down here.

where it's You know it hasn't really increased in temperature much since here, but yeah, like it's You know it's been tracking there because that's been the temperature here. In like the building and you know, the corridor. It seeps in through the roof, the walls, everything else. So I've had some slight temperature variations here, but looks like it's reaching a new low there.
and this brings up interesting things in, you know, long-term trend plot in Wicked Me, you know, plot. This thing for two weeks in a temperature chamber and stable and everything else and we might see some drift. And you know things like that, It might you know, settle down and you know all that sort of jazz when you're talking about the the precision, the resolution we're looking at here and all the little subtle things, matter and long-term aging and and drift and other. You know they could even be some sort of, you know, quantum effects in the reference or whether you might like weird, you know, a physical phenomenon at play in you know it could be fascinating stuff if you leave it for weeks and months.

And you know some people leave them for years to see the long-term drift in things that can be absolutely fascinating. So there you go I wonder where it's going to go? But yeah I think I'm gonna call it quits now. you.

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By YTB

23 thoughts on “Eevblog #835 – wekomm resistance standard part 2”
  1. Avataaar/Circle Created with python_avatars CoolMusicToMyEars says:

    Your Noise might come from the Fluorescent Lights, But I be honest Dave, if you use far better cables, use guard if Keithley has it to the Resistor case, isolate from anything that the case might touch,
    Use Raychem PTFE Insulated Silver Plated Copper Twisted Pair, Silver plated Copper Screen, outer Tufnel Coating, use one for sense & one for Input, spades Gold plated copper Spades, crimped on each end of lead,
    You might need an EMC Sniffer Probe to look at the area for noise pickup, use mass in the thermal chamber for better stability, Don't forget you have plated test connectors nickel which is not that good for good mesurements,
    I would love to see a Solartron 7081 DMM thats really great for its age ๐Ÿ™‚ or a Datron 1081 if you use better cables far better results,

  2. Avataaar/Circle Created with python_avatars Question Mark says:

    Thank you, Dave, for letting us participate in this truly fascinating two part test. Super interesting and please keep doing this sort of videos!
    Cheers
    Mark

  3. Avataaar/Circle Created with python_avatars feasibletrash0 says:

    "one does not just measure the stability of a resistance standard"

  4. Avataaar/Circle Created with python_avatars Jacob Feder says:

    Maybe the noise is nyquist aliasing? E.g. you could have 50Hz or some higher switching frequency picked up from the leads folding back into your measurement.

  5. Avataaar/Circle Created with python_avatars Djordje Lukovac says:

    Oh,please Dave,we are not in NASA.

  6. Avataaar/Circle Created with python_avatars Dennis Lubert says:

    A quick tuning of that "thermal chamber" could be done by getting some big cpu cooler with heatpipes (like thermaltake macho I did mine with) and some cheap ebay peltier element that has some more wattage (120 or so) and some internal fan and good heatsink there too. This should be able to pump out the 10W of the meter too.

  7. Avataaar/Circle Created with python_avatars Christopher de Villiers says:

    The thermal chamber looks like a mini fridge to me

  8. Avataaar/Circle Created with python_avatars Red Squirrel says:

    We need to get audiophiles in on this concept, perhaps there is a market for oven controlled audio cables, so the entire length of the cable is kept at a stable temperature, to keep a steady resistance.

  9. Avataaar/Circle Created with python_avatars AM Jasin says:

    Thank you ! Excellent channel. Happy New Year. As a gift if you do not know yet I think really interesting channels: reduktor szumu (noice reductor) and RS elektronika – it is in polish but I think you will like some. All the best from Poland and once again congratulate really nice channel.

  10. Avataaar/Circle Created with python_avatars david jones says:

    make siure your oven is at the correct temp

  11. Avataaar/Circle Created with python_avatars david jones says:

    nit piiking

  12. Avataaar/Circle Created with python_avatars Jerry Walker says:

    Totally agree with reburneI see this a lot and it is generally caused by the mismatched materials in the leads / instrument terminals. This can contribute large affects at these measurement levels.The sudden dips when switching on the air con may just be the leads changing temp quickly compared to the meter terminals.

  13. Avataaar/Circle Created with python_avatars RC Hobbyist Extreme says:

    what brand power regulator do you recommend for hobby grade use. I want one to use for testing led and R/c plane use. I work with of course leds and servo's as well as other electronic equipment.I see plenty of cheapy units available on ebay. what do you think.

  14. Avataaar/Circle Created with python_avatars KX36 says:

    An oscillation with a period of 500s when the "thermal chamber" (I vaguely remember it is a hacked mini fridge …?) is in use is almost certainly due to oscillating temperatures within the chamber. I haven't watched your vid on that since it was new but most temperature control loops have significant hysteresis which causes low frequency oscillation. It's acceptable in a fridge, AC etc as long as the amplitude of oscillation is relatively low (amplitude may also change depending on position within the chamber). Even though there is some small amount of thermal damping from the case around the resistor, I think it still must be that you're seeing (probably thermocouple effect at the jacks). The AC appears to have a longer period of oscillation.

    Also, I feel uneasy when you say you've "proven" something. You can't really prove anything with 1 measurement. e.g when you say you've "proven" the temp co of the meter is negative, really what you mean is you have some evidence to suggest it's NTC within this temperature range.

  15. Avataaar/Circle Created with python_avatars Peter Walker says:

    You obviously need to invest in some audiophool unobtanium plated leads, connectors, enclosures and whatnot.

  16. Avataaar/Circle Created with python_avatars metaforest says:

    I think Dave is right… Without shielded leads between the Resistor ref and the meter…. the High Freq. (relative to the larger trends) noise is most likely the temp-chamber due to EMI, and not from thermal noise in either the room or the chamber. I think his turning off both the A/C and T/C show where the noise floor really is for the situation.

  17. Avataaar/Circle Created with python_avatars movax20h says:

    It is a radiator on a back of a thermal chamber radiating heat and interfering with the meter. Try putting chamber further away from the meter, put the meter in front of the chamber instead. There might also be some induction from the chamber motor, or something else creating some residual currents in leads.

  18. Avataaar/Circle Created with python_avatars es nam says:

    The last two videos are really neat and intersting. Thank you very much Dave.

  19. Avataaar/Circle Created with python_avatars Tricky D says:

    Come on Dave, tear something apart!

  20. Avataaar/Circle Created with python_avatars iceberg789 says:

    can we get a hour or two long video on inductors also ?

  21. Avataaar/Circle Created with python_avatars Dave Blane says:

    What an utter waste of time.

  22. Avataaar/Circle Created with python_avatars Cisco8484 says:

    I wonder if your wife knows you used her shirt as a rag?

  23. Avataaar/Circle Created with python_avatars vitor de miranda henrique says:

    Can I use those super-precise resistors as pull up resistors on my arduino projects? ๐Ÿ˜›

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